Single source precursor routes for synthesis of PdTe nanorods and particles: solvent dependent control of shapes.
نویسندگان
چکیده
The PdTe NPs (hexagonal) and nanorods (first example) have been synthesized for the first time from single source precursors (SSPs), [Pd(L1)Cl2] (1) and [Pd(L2)Cl]BF4 (2) [L1, 4-bromo-1-[2-(4-methoxyphenyltellanyl)ethyl]-1H-pyrazole; L2, bis-[2-(4-bromopyrazol-1-yl)ethyl]telluride], by their thermolysis in an OA–ODE mixture (1:1) and TOP respectively. The composition of the PdTe phase does not change with SSP/solvent. Complex 2 gives small size nanostructures.
منابع مشابه
PVP-Assisted Synthesis of Cobalt Ferrite (CoFe2O4) Nanorods
Cobalt ferrite (CoFe2O4) nanorods were synthesized by iron chloride (FeCl3.6H2O) and cobalt sulfate hexahydrate (CoSO4.7H2O) as precursor in the presence of ethylene glycol agent and poly vinyl pyrrolidone (PVP) surfactant. The samples were characterized to identify the physical properties. XRD pattern of cobalt ...
متن کاملNew Dinuclear Methoxo-Bridged Manganese(III) complex: Synthesis, Characterization and Usage as New Precursor for Synthesis of Mn2O3 Particles
New dinuclear methoxo-bridged manganese(III) complex [Mn2((MeO-bph)en)2Cl2(m-CH3O)2] (1) was synthesized by template reaction of 2-hydroxy-4-methoxybenzophenone, 1,2-ethanediamine and MnCl2×6H2O with molar ration (1:1:1) in methanol as solvent. The title compound 1 was characterized by...
متن کاملMicrowave-assisted rapid synthesis of Co3O4 nanorods from CoC2O4.2H2O nanorods and its application in photocatalytic degradation of methylene blue under visible light irradiation
In this work, Co3O4 nanorods were successfully prepared by microwave-assisted solid state decomposition of rod-like CoC2O4.2H2O precursor within a very short reaction time (6 min) without the use of a solvent/surfactant and complicated equipment. The as-obtained Co3O4 nanorods were fully characterized by X-ray diffract...
متن کاملFabrication and Characterization of Nanoporous Co Oxide (Co3O4) Prepared by Simple Sol-gel Synthesis
Cobalt oxide (Co3O4) nanorods were prepared by a simple co-precipitation method using ethanol solution of cobalt nitrate as precursor and cetyl trimethylammonium bromide (CTAB) as surfactant. Morphological properties of the nanoparticles were characterized. XRD measurement exhibited the structure of Co3O4 nanocrystals for annealed samples. The SEM ima...
متن کاملMicrowave-assisted rapid synthesis of Co3O4 nanorods from CoC2O4.2H2O nanorods and its application in photocatalytic degradation of methylene blue under visible light irradiation
In this work, Co3O4 nanorods were successfully prepared by microwave-assisted solid state decomposition of rod-like CoC2O4.2H2O precursor within a very short reaction time (6 min) without the use of a solvent/surfactant and complicated equipment. The as-obtained Co3O4 nanorods were fully characterized by X-ray diffract...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید
ثبت ناماگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید
ورودعنوان ژورنال:
- Chemical communications
دوره 49 81 شماره
صفحات -
تاریخ انتشار 2013